Fe–based metallic microwires possess unique microstructure and size effects, exhibiting favorable mechanical, electrical, and magnetic properties, thus distinguishing them as a possible agents for use as microwave absorbing materials. In this paper, the absorbing properties of Ni– doped Fe–based metallic microwires optimized by orthogonal experiments were investigated, and based on the optimal parameters, the influencing mechanism of the Ni doping amount on the absorbing properties was further analyzed. It was noted that at the frequency f = 8.36 GHz, the maximum reflection loss RL and electromagnetic wave absorption efficiency Aeff can reach −54.89 dB and 99.999%, respectively. Moreover, the Ni doping amount could result in the improved Waveabsorbing properties of composites, obtain the corresponding optimal parameters, and even change the position of the maximum absorption peak, which are all of great significance for practical engineering applications.
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